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Dynamic Leach Analysis
Harvel LXT® piping has been subjected to on-line dynamic flow analysis with 18.2 megohm UPW to evaluate particles, TOC, resistivity, anions, cations, and trace metals. This testing utilized solvent-cemented flange assemblies (spool piece) to see the effect that the cement had on TOC, resistivity and particle generation in a freshly assembled pipe section. Grab samples were also pulled periodically (at start-up, five minutes, 50 minutes and five hours) to analyze anions, cations and trace metals under flowing conditions. Harvel LXT® Flanges were assembled utilizing Harvel LXT® One-Step Cement and allowed to cure 24 hours prior to testing. Dynamic testing revealed that Harvel LXT® piping assemblies did not contribute significantly to particle generation or leachable contamination under flowing conditions throughout the test duration. Additional detailed information is available from Harvel.
Dynamic Test Description
Ambient temperature dynamic leach utilizing 18.2 megohm UPW flowing at 9.35 GPM (turbulent flow). 1" diameter pipe 30" long, solvent-cemented flanges each end (approximately 82-square-inch wet surface contact area). Approximately 1-1/2 grams of Harvel LXT® solvent cement used in assembly of components. Solvent-cemented assembly was allowed to cure 24 hours prior to start-up. Dynamic test was conducted for a period of five hours.
Resistivity
Resistivity measured 17.95 megohms at the start of the leach and rose quickly to 18.12 megohms during the first 6 minutes. Resistivity readings continued to rise until reaching the background level of 18.2 megohms after five hours of leaching. |
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Total Oxidizable Carbon (TOC)
Dynamic testing revealed that after four hours of leaching, TOC readings reached and maintained the background levels throughout the test duration. This data confirmed the fast cure time of Harvel LXT® One-Step Cement. Conventional solvent cements and primers used for joining typically effect TOC contamination as a result of the leach. |
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Particles
Dynamic testing revealed that average particle counts decreased rapidly during the first six minutes of the leach. After 12 minutes of leaching the average smallest particles measured (0.05 micron size range) were representative of the background levels. |
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Leachable Contamination
Anions/Cations IC grab sample analysis revealed low levels of sulfate (0.15 ppb) five minutes into the test, and low levels of ammonium at 50 minutes (0.05 ppb) and five hours (0.07ppb) into the test. All other IC contaminants were below the limit of detection.
Trace Metals Of the 68 trace metal contaminants evaluated, all were below the limit of detection with the exception of aluminum, detected at 0.012 ppb at the five-minute interval. This element remained below the limit of detection throughout the remainder of the leach.
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